X-ray crystal structure and theoretical analysis of Au 25- xAgx(SCH2CH2Ph) 18- alloy

Chanaka Kumara, Christine M. Aikens, Amala Dass

Research output: Contribution to journalArticlepeer-review

214 Scopus citations

Abstract

The atomic arrangement of Au and Ag atoms in Au25-xAg x(SR)18 was determined by X-ray crystallography. Ag atoms were selectively incorporated in the 12 vertices of the icosahedral core. The central atom and the metal atoms in the six [-SR-Au-SR-Au-SR-] units were exclusively gold, with 100% Au occupancy. The composition of the crystals determined by X-ray crystallography was Au18.3Ag 6.7(SCH2CH2Ph)18. This composition is in reasonable agreement with the composition Au18.8Ag 6.2(SCH2CH2Ph)18 measured by electrospray mass spectrometry. The structure can be described in terms of shells as Au1@Au5.3Ag6.7@6×[-SR-Au-SR-Au- SR-]. Density functional theory calculations show that the electronic structure and optical absorption spectra are sensitive to the silver atom arrangement within the nanocluster.

Original languageEnglish
Pages (from-to)461-466
Number of pages6
JournalJournal of Physical Chemistry Letters
Volume5
Issue number3
DOIs
StatePublished - Feb 6 2014
Externally publishedYes

Funding

FundersFunder number
National Science FoundationEPS-0919443, CHE-1213771, EPS-1006860, CHE-1255519, CNS-1006860
National Science Foundation
Directorate for Mathematical and Physical Sciences1213771, 1255519

    Keywords

    • Au
    • alloy nanomolecules
    • gold-silver alloy
    • monolayer protected clusters

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