TY - JOUR
T1 - When x-rays alter the course of your experiments
AU - Bras, Wim
AU - Myles, Dean A.A.
AU - Felici, Roberto
N1 - Publisher Copyright:
© 2021 Institute of Physics Publishing. All rights reserved.
PY - 2021/10
Y1 - 2021/10
N2 - The continuing increase in the brilliance of synchrotron radiation beamlines allows for many new and exciting experiments that were impossible before the present generation of synchrotron radiation sources came on line. However, the exposure to such intense beams also tests the limits of what samples can endure.Whilst the effects of radiation induced damage in a static experiment often can easily be recognized by changes in the diffraction or spectroscopy curves, the influence of radiation on chemical or physical processes, where one expects curves to change, is less often recognized and can be misinterpreted as a 'real' result instead of as a 'radiation influenced result'. This is especially a concern in time-resolved materials science experiments using techniques as powder diffraction, small angle scattering and x-ray absorption spectroscopy. Here, the effects of radiation (5-50 keV) on some time-resolved processes in different types of materials and in different physical states are discussed. We show that such effects are not limited to soft matter and biology but rather can be found across the whole spectrum of materials research, over a large range of radiation doses and is not limited to very high brilliance beamlines 2021 IOP Publishing Ltd.
AB - The continuing increase in the brilliance of synchrotron radiation beamlines allows for many new and exciting experiments that were impossible before the present generation of synchrotron radiation sources came on line. However, the exposure to such intense beams also tests the limits of what samples can endure.Whilst the effects of radiation induced damage in a static experiment often can easily be recognized by changes in the diffraction or spectroscopy curves, the influence of radiation on chemical or physical processes, where one expects curves to change, is less often recognized and can be misinterpreted as a 'real' result instead of as a 'radiation influenced result'. This is especially a concern in time-resolved materials science experiments using techniques as powder diffraction, small angle scattering and x-ray absorption spectroscopy. Here, the effects of radiation (5-50 keV) on some time-resolved processes in different types of materials and in different physical states are discussed. We show that such effects are not limited to soft matter and biology but rather can be found across the whole spectrum of materials research, over a large range of radiation doses and is not limited to very high brilliance beamlines 2021 IOP Publishing Ltd.
KW - Material science
KW - Radiation interactions
KW - Synchrotron radiation
KW - Time-resolved experiments
UR - http://www.scopus.com/inward/record.url?scp=85112605378&partnerID=8YFLogxK
U2 - 10.1088/1361-648X/ac1767
DO - 10.1088/1361-648X/ac1767
M3 - Review article
C2 - 34298526
AN - SCOPUS:85112605378
SN - 0953-8984
VL - 33
JO - Journal of Physics Condensed Matter
JF - Journal of Physics Condensed Matter
IS - 42
M1 - 423002
ER -