TY - JOUR
T1 - Two-dimensional camera for millisecond range time-resolved small-and wide-angle X-ray scattering
AU - Urban, Volker
AU - Panine, Pierre
AU - Ponchut, Cyril
AU - Boesecke, Peter
AU - Narayanan, Theyencheri
PY - 2003
Y1 - 2003
N2 - A combined small-angle and wide-angle X-ray scattering (SAXS/WAXS) camera has been implemented using area detectors suitable for real time experiments down to millisecond time range. The design is based on the existing high brilliance SAXS camera with a sample-to-detector distance variable from 1 m to 10 m and to which a two-dimensional WAXS detector is coupled. Two independent image intensified CCD detectors allow simultaneous real-time SAXS/WAXS experiments on oriented samples down to the millisecond time range. A wide scattering vector range spanning from 0.001 Å-1 to 6 Å-1 is covered by this combined setup. Both detectors have single photon sensitivity and the spatial resolution is about 200 pm. The WAXS detector is mounted at an angle inclined to the primary beam and the process of image transformation into non-arbitrary scattering vector coordinates is demonstrated for a standard p-bromobenzoic acid sample.
AB - A combined small-angle and wide-angle X-ray scattering (SAXS/WAXS) camera has been implemented using area detectors suitable for real time experiments down to millisecond time range. The design is based on the existing high brilliance SAXS camera with a sample-to-detector distance variable from 1 m to 10 m and to which a two-dimensional WAXS detector is coupled. Two independent image intensified CCD detectors allow simultaneous real-time SAXS/WAXS experiments on oriented samples down to the millisecond time range. A wide scattering vector range spanning from 0.001 Å-1 to 6 Å-1 is covered by this combined setup. Both detectors have single photon sensitivity and the spatial resolution is about 200 pm. The WAXS detector is mounted at an angle inclined to the primary beam and the process of image transformation into non-arbitrary scattering vector coordinates is demonstrated for a standard p-bromobenzoic acid sample.
KW - Small-angle scattering
KW - Time-resolved studies
KW - Wide-angle scattering
UR - http://www.scopus.com/inward/record.url?scp=0037701576&partnerID=8YFLogxK
U2 - 10.1107/S0021889803000554
DO - 10.1107/S0021889803000554
M3 - Article
AN - SCOPUS:0037701576
SN - 0021-8898
VL - 36
SP - 809
EP - 811
JO - Journal of Applied Crystallography
JF - Journal of Applied Crystallography
IS - 3 I
ER -