Thermorheological studies of plasticized polyvinylchloride filled with ground rubber tire and its chlorinated derivative

A. K. Naskar, D. P. Gala, S. K. De, A. K. Bhowmick

Research output: Contribution to journalArticlepeer-review

7 Scopus citations

Abstract

Ground rubber tire (GRT) and its chlorinated derivative (CI-GRT) were filled in a plasticized polyvinylchloride (PVC) compound. Thermorheological studies of the PVC compound and its blends with GRT and CI-GRT were done using a shear dynamic oscillating rheometer. Rheological complexity of the compositions was analyzed from double logarithmic plot of storage modulus (G′) and loss modulus (G″). Log-log plot of complex shear viscosity (η*) and its real component (η′) against frequency (ω) revealed higher degree of interaction between CI-GRT and PVC compared to that between GRT and PVC. Activation energy for the flow of the PVC/CI-GRT blend was lower than that of the PVC/GRT blend indicating retention of the network structure of the former during flow; whereas for the later lower viscosity and hence higher free volume enabled it to loose entanglement by shear force at higher temperature. PVC/CI-GRT blend exhibited lower die swell and better extrutdate surface smoothness than those of PVC/GRT blend, when extruded at a shear rate of 900 s-1.

Original languageEnglish
Pages (from-to)164-168
Number of pages5
JournalKGK-Kautschuk und Gummi Kunststoffe
Volume55
Issue number4
StatePublished - Apr 2002
Externally publishedYes

Keywords

  • Activation energy for flow
  • Chlorinated ground rubber tire
  • Extrusion characteristics
  • Ground rubber tire
  • Polyvinylchloride
  • Thermorheological analysis

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