Abstract
An atom probe tomography microstructural characterization has been performed on an A533B pressure vessel steel (JRQ) after irradiation to a fluence of 5 × 1023 n m-2 (E > 1 MeV) and a subsequent annealing treatment of 168 h at 460 °C and also through two cycles of neutron irradiation (0.85 × 1023 n m-2 (E > 1 MeV)) and annealing (168 h at 460 °C). The alloy that was neutron irradiated to a fluence of 5 × 1023 n m-2 exhibited a high number density of Cu-enriched precipitates and a shift in the ductile-to-brittle transformation temperature of ΔT41J = 96 °C. Annealing for 168 h at 460 °C coarsened these Cu-enriched precipitates and recovered the embrittlement. The material that was re-irradiated to a total fluence 1.7 × 1023 n m-2 also exhibited a high number density of Cu-enriched precipitates and a ΔT41J shift of 56 °C. Annealing the re-irradiated material for 168 h at 460 °C coarsened these precipitates and recovered the embrittlement.
Original language | English |
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Pages (from-to) | 216-222 |
Number of pages | 7 |
Journal | Journal of Nuclear Materials |
Volume | 351 |
Issue number | 1-3 |
DOIs | |
State | Published - Jun 1 2006 |
Funding
The authors would like to thank Drs R. Dietmar Kalkhof and Markus Niffenegger of the Paul Scherrer Institute, Switzerland and Philip Tipping of the Swiss Federal Nuclear Safety Inspectorate for their significant contributions to the research presented in this paper. Research at the Oak Ridge National Laboratory SHaRE User Facility was sponsored by the Division of Materials Sciences and Engineering (atom probe), US Department of Energy, under contract DE-AC05-00OR22725 with UT-Battelle, LLC and by the Office of Nuclear Regulatory Research, US Nuclear Regulatory Commission under inter-agency agreement DOE 1886-N695-3W with the US Department of Energy.
Funders | Funder number |
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Office of Nuclear Regulatory Research | |
US Department of Energy | DE-AC05-00OR22725 |
U.S. Nuclear Regulatory Commission | |
Division of Materials Sciences and Engineering |
Keywords
- A0800
- P1200
- R0200