The crystal structure and phase transition of sulphamide by high-resolution neutron powder diffraction

R. M. Ibberson

doi:10.1016/0022-2860(95)09128-9

The crystal structure and phase transition of sulphamide by high-resolution neutron powder diffraction

R. M. Ibberson

Research output: Contribution to journal › Article › peer-review

7 Scopus citations

Abstract

Detailed crystal structure analyses of natural, SO₂ (NH₂)₂, and perdeuterated sulphamide have been carried out at 5 K. and 293 K using high-resolution neutron powder diffraction data. Earlier spectroscopic evidence of a pre-melting transition has been confirmed by investigations of the evolution of the crystal structure between ambient temperature and the melting point at 363.5 K.

Original language	English
Pages (from-to)	171-179
Number of pages	9
Journal	Journal of Molecular Structure
Volume	377
Issue number	2
DOIs	https://doi.org/10.1016/0022-2860(95)09128-9
State	Published - 1996
Externally published	Yes

Keywords

Neutron powder diffraction
Phase transition
Sulphamide

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10.1016/0022-2860(95)09128-9

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title = "The crystal structure and phase transition of sulphamide by high-resolution neutron powder diffraction",

abstract = "Detailed crystal structure analyses of natural, SO2 (NH2)2, and perdeuterated sulphamide have been carried out at 5 K. and 293 K using high-resolution neutron powder diffraction data. Earlier spectroscopic evidence of a pre-melting transition has been confirmed by investigations of the evolution of the crystal structure between ambient temperature and the melting point at 363.5 K.",

keywords = "Neutron powder diffraction, Phase transition, Sulphamide",

author = "Ibberson, {R. M.}",

year = "1996",

doi = "10.1016/0022-2860(95)09128-9",

language = "English",

volume = "377",

pages = "171--179",

journal = "Journal of Molecular Structure",

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publisher = "Elsevier",

number = "2",

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T1 - The crystal structure and phase transition of sulphamide by high-resolution neutron powder diffraction

AU - Ibberson, R. M.

PY - 1996

Y1 - 1996

N2 - Detailed crystal structure analyses of natural, SO2 (NH2)2, and perdeuterated sulphamide have been carried out at 5 K. and 293 K using high-resolution neutron powder diffraction data. Earlier spectroscopic evidence of a pre-melting transition has been confirmed by investigations of the evolution of the crystal structure between ambient temperature and the melting point at 363.5 K.

AB - Detailed crystal structure analyses of natural, SO2 (NH2)2, and perdeuterated sulphamide have been carried out at 5 K. and 293 K using high-resolution neutron powder diffraction data. Earlier spectroscopic evidence of a pre-melting transition has been confirmed by investigations of the evolution of the crystal structure between ambient temperature and the melting point at 363.5 K.

KW - Neutron powder diffraction

KW - Phase transition

KW - Sulphamide

UR - http://www.scopus.com/inward/record.url?scp=0039814797&partnerID=8YFLogxK

U2 - 10.1016/0022-2860(95)09128-9

DO - 10.1016/0022-2860(95)09128-9

M3 - Article

AN - SCOPUS:0039814797

SN - 0022-2860

VL - 377

SP - 171

EP - 179

JO - Journal of Molecular Structure

JF - Journal of Molecular Structure

IS - 2

ER -

The crystal structure and phase transition of sulphamide by high-resolution neutron powder diffraction

Abstract

Keywords

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