Temperature dependent deformation mechanisms in pure amorphous silicon

M. S.R.N. Kiran, B. Haberl, J. S. Williams, J. E. Bradby

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9 Scopus citations

Abstract

High temperature nanoindentation has been performed on pure ion-implanted amorphous silicon (unrelaxed a-Si) and structurally relaxed a-Si to investigate the temperature dependence of mechanical deformation, including pressure-induced phase transformations. Along with the indentation load-depth curves, ex situ measurements such as Raman micro-spectroscopy and cross-sectional transmission electron microscopy analysis on the residual indents reveal the mode of deformation under the indenter. While unrelaxed a-Si deforms entirely via plastic flow up to 200°C, a clear transition in the mode of deformation is observed in relaxed a-Si with increasing temperature. Up to 100°C, pressure-induced phase transformation and the observation of either crystalline (r8/bc8) end phases or pressure-induced a-Si occurs in relaxed a-Si. However, with further increase of temperature, plastic flow rather than phase transformation is the dominant mode of deformation. It is believed that the elevated temperature and pressure together induce bond softening and "defect"formation in structurally relaxed a-Si, leading to the inhibition of phase transformation due to pressure-releasing plastic flow under the indenter.

Original languageEnglish
Article number113511
JournalJournal of Applied Physics
Volume115
Issue number11
DOIs
StatePublished - Mar 21 2014
Externally publishedYes

Funding

FundersFunder number
Australian Research Council

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