Synthesis of nanocrystalline BaTiO3 by solvent refluxing method

X. Wang; B. I. Lee; M. Z. Hu; E. A. Payzant; D. A. Blom

doi:10.1023/A:1022907024179

Synthesis of nanocrystalline BaTiO₃ by solvent refluxing method

X. Wang, B. I. Lee, M. Z. Hu, E. A. Payzant, D. A. Blom

Materials Engineering

Research output: Contribution to journal › Article › peer-review

17 Scopus citations

Abstract

Nanocrystalline BaTiO₃ particles in various media were synthesized by a refluxing method. It was found that BaTiO₃ nanocrystals can be formed by refluxing of precursor precipitate in toluene, n-butanol, tert-amyl alcohol and water. These nanocrystals were identified as metastable cubic phase BaTiO₃ by X-ray diffraction and FT-Raman. FTIR data shows that BaTiO₃ powders prepared in non-aqueous refluxing media have less -OH content.

Original language	English
Pages (from-to)	557-559
Number of pages	3
Journal	Journal of Materials Science Letters
Volume	22
Issue number	7
DOIs	https://doi.org/10.1023/A:1022907024179
State	Published - Apr 1 2003

Funding

This work is sponsored by the Division of Materials Science, Office of Basic Energy Sciences, of the U.S. Department of Energy, and partially sponsored by NSF DMR-9731769. Research is also sponsored in part by the Assistant Secretary for Energy Efficiency and Renewable Energy, Office of Transportation Technologies, as part of the High Temperature Materials Laboratory User Program, Oak Ridge National Laboratory, managed by UT-Battelle, LLC, for the U.S. Dept. of Energy under contract DE-AC05-00OR22725.

Funders	Funder number
Office of Transportation Technologies
National Science Foundation	DMR-9731769
U.S. Department of Energy	DE-AC05-00OR22725
Office of Energy Efficiency and Renewable Energy
Basic Energy Sciences
Oak Ridge National Laboratory
Division of Materials Sciences and Engineering

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abstract = "Nanocrystalline BaTiO3 particles in various media were synthesized by a refluxing method. It was found that BaTiO3 nanocrystals can be formed by refluxing of precursor precipitate in toluene, n-butanol, tert-amyl alcohol and water. These nanocrystals were identified as metastable cubic phase BaTiO3 by X-ray diffraction and FT-Raman. FTIR data shows that BaTiO3 powders prepared in non-aqueous refluxing media have less -OH content.",

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AU - Lee, B. I.

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AU - Payzant, E. A.

AU - Blom, D. A.

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AB - Nanocrystalline BaTiO3 particles in various media were synthesized by a refluxing method. It was found that BaTiO3 nanocrystals can be formed by refluxing of precursor precipitate in toluene, n-butanol, tert-amyl alcohol and water. These nanocrystals were identified as metastable cubic phase BaTiO3 by X-ray diffraction and FT-Raman. FTIR data shows that BaTiO3 powders prepared in non-aqueous refluxing media have less -OH content.

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Synthesis of nanocrystalline BaTiO₃ by solvent refluxing method

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