Abstract
High-resolution powder neutron diffraction has been used to study the crystal structure of the Mg11B2 superconductor (Tc = 39.2 K) prepared at high pressure in the temperature range 2 to 293 K. The experimental data provide clear evidence of temperature-independent phase inhomogeneity, which was modelled by coexisting Mg1+δB2 phases. Precise structural information for temperatures near Tc also reveals extremely small volume and c-axis discontinuities, consistent with the existence of a specific heat anomaly at Tc.
| Original language | English |
|---|---|
| Pages (from-to) | L795-L802 |
| Journal | Journal of Physics Condensed Matter |
| Volume | 13 |
| Issue number | 35 |
| DOIs | |
| State | Published - Sep 3 2001 |
| Externally published | Yes |