Abstract
While laser powder-bed fusion has overcome some of the design constraints of conventional manufacturing methods, it requires careful selection of process parameters and scan strategies to obtain favorable properties. Here we show that even simple scan strategies, complex ones being inevitable when printing intricate designs, can inadvertently produce local alterations of the microstructure and preferential grain orientation over small areas – which easily remain unnoticed across the macroscale. We describe how a combined usage of neutron imaging and electron backscatter diffraction can reveal these localized variations and explain their origin within cm-sized parts. We explain the observed contrast variations by linking the neutron images to simulated data, pole figures and EBSD, providing an invaluable reference for future studies and showing that presumably minor changes of the scan strategy can have detrimental effects on the mechanical properties. In-situ tensile tests reveal that fracture occurs in a region that was re-melted during the building process.
Original language | English |
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Article number | 101614 |
Journal | Materialia |
Volume | 26 |
DOIs | |
State | Published - Dec 2022 |
Funding
This research is funded by the Swedish Foundation for Strategic Research (SSF) within the Swedish national graduate school in neutron scattering (SwedNess) and by the Swedish Foundation for Strategic Research (SSF), through the project “SSF − Development of processes and Materials in AM”. This work was also supported by OP RDE MEYS, under the project “ European Spallation Source – participation of the Czech Republic – OP ”, Reg. No. CZ.02.1.01/0.0/0.0/16013/0001794. Measurements were carried out at the CONRAD 2 instrument at Helmholtz-Zentrum Berlin für Materialien und Energie (HZB). The authors wish to thank Dr Ashok Menon, Dr Malcolm Guthrie and Dr Rebecca Clulow for proofreading our manuscript. The authors wish to thank Dr Alexandru A. Stoica for his guidance on the simulations. Dr Luc Dessieux acknowledges support at Oak Ridge National Laboratory from the US DOE Office of Scientific User facilities. This research is funded by the Swedish Foundation for Strategic Research (SSF) within the Swedish national graduate school in neutron scattering (SwedNess) and by the Swedish Foundation for Strategic Research (SSF), through the project “SSF − Development of processes and Materials in AM”. This work was also supported by OP RDE MEYS, under the project “European Spallation Source – participation of the Czech Republic – OP”, Reg. No. CZ.02.1.01/0.0/0.0/16013/0001794. Measurements were carried out at the CONRAD 2 instrument at Helmholtz-Zentrum Berlin für Materialien und Energie (HZB). The authors wish to thank Dr Ashok Menon, Dr Malcolm Guthrie and Dr Rebecca Clulow for proofreading our manuscript. The authors wish to thank Dr Alexandru A. Stoica for his guidance on the simulations. Dr Luc Dessieux acknowledges support at Oak Ridge National Laboratory from the US DOE Office of Scientific User facilities.
Keywords
- Bragg-edge
- Diffraction contrast neutron imaging
- Inhomogeneous microstructure
- Laser powder-bed fusion
- Preferential orientation
- Texture
- Texture control