On the bulk compaction of brittle granular materials, part I: SeS analysis of axial compression to 4000 MPa*

  • Andrew A. Wereszczak
  • , Madeline D. Loveday
  • , Emily F. Ghezawi
  • , Kristopher V. Jones
  • , Nicodemus A. Rod
  • , Stephen C. Hyde
  • , Samantha J. Kotze

Research output: Contribution to journalArticlepeer-review

2 Scopus citations

Abstract

The bulk compaction of granular materials has been studied for decades to interpret and manage responses for soils and powder-based component fabrication, and geophysical, celestial, and ballistic impact. Their bulk or macroscopic compaction response is limited by what occurs at the granular or microstructural scale. Motivation existed to more closely examine that association specific to granular brittle materials (e.g., ceramics and glasses). That examination is offered in a series of three companion papers where Part I describes a new supplemental analysis adopted to bulk compaction response involving relatively high compaction stresses (4000 MPa). Bulk compactions of vitreous silicates and crystalline quartzes were interpreted in three ways, including that of a new analysis that considers the product of void ratio (e) and stress (S) as a function of S, hereafter referred to as “SeS analysis”. The SeS analysis was found to be an informative supplement to conventional bulk compaction analyses because it provides more consistent higher sensitivity for the identification of bulk density rate increase with increasing compaction (softening); a rate increase that arises from the cumulative effect of the onsets and progression of compaction-induced yielding, fracture or comminution, densification, phase change, or combinations thereof occurring at the granular or microstructural scale.

Original languageEnglish
Article numbere70076
JournalInternational Journal of Applied Ceramic Technology
Volume23
Issue number1
DOIs
StatePublished - Feb 2026

Funding

The authors thank Oak Ridge National Laboratory's (ORNL's) B. Cowell for financial and technical influences, Applied Research Associates's D. Grady and National Institute of Standards and Technology's G. Quinn (Emeritus) and Alfred University's W. Carty (Emeritus) for insights and inputs, University of Tennessee's N. Smith, M. Sereno, J. Dahlhauser, A. Guariglia, R. Parten, for their technical support, the University of Tennessee's Institute for Advanced Materials and Manufacturing Diffraction Facility's M. Koehler for assistance with XRD, Johns Hopkins University's B. Kuwik for providing the Ottawa sand, and ORNL's M. Ciccarella for conducting colorimetry measurements, and D. Delia, M. Modugno, and J. Hemrick for their technical reviews of this manuscript.

Keywords

  • compaction
  • crystalline quartz
  • stress
  • vitreous silicate
  • void ratio

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