Microstructure and high temperature properties of tungsten processed via electron beam melting additive manufacturing

Christopher Ledford, Patxi Fernandez-Zelaia, Tim Graening, Quinn Campbell, Julio Ortega Rojas, Andrés Márquez Rossy, Yutai Kato, Michael M. Kirka

Research output: Contribution to journalArticlepeer-review

17 Scopus citations

Abstract

There is considerable interest in the adoption of additive manufacturing for processing refractory metals. The layer-wise fabrication approach enables opportunities for producing complex geometries which cannot be otherwise be achieved via powder metallurgy. However, the processing science is still in its nascent stages and structure–property relations are relatively unexplored. Fundamental research is needed to further develop the technology and enable the fabrication of refractory metals for high temperature applications. Here we focus on the processing of pure tungsten using electron beam melting additive manufacturing. Experimentally we develop a suitable processing window for achieving high density crack free material. Microstructural analysis reveals that the microstructure generally consists of a columnar structure with a 111 build direction fiber preference, although, fiber switching was observed. Process induced deformation is believed to drive the formation of subgrains whose boundaries exhibit a high dislocation density. High temperature tensile testing reveals that the material exhibits excellent properties closer to that of annealed tungsten. Significant mechanical anisotropy was observed to be present which is likely driven by strong crystallographic texture.

Original languageEnglish
Article number106148
JournalInternational Journal of Refractory Metals and Hard Materials
Volume113
DOIs
StatePublished - Jun 2023

Funding

This research was sponsored by the US Department of Energy, Office of Fusion Energy Sciences and Advanced Research Projects Agency- Energy (ARPA-E) under contract DE-AC05–00OR22725 with UT- Battelle LLC. In addition, work was performed at Oak Ridge National Laboratory's Manufacturing Demonstration Facility, an Office of Energy Efficiency and Renewable Energy user facility. All microscopy presented in this work was performed with the support of Carl Zeiss via a cooperative research and development agreement (NFE-19–07705). This research was sponsored by the US Department of Energy, Office of Fusion Energy Sciences and Advanced Research Projects Agency- Energy (ARPA-E) under contract DE-AC05–00OR22725 with UT- Battelle LLC. In addition, work was performed at Oak Ridge National Laboratory’s Manufacturing Demonstration Facility, an Office of Energy Efficiency and Renewable Energy user facility. All microscopy presented in this work was performed with the support of Carl Zeiss via a cooperative research and development agreement (NFE-19–07705). Notice of Copyright . This manuscript has been authored by UT-Battelle, LLC under Contract No. DE-AC05-00OR22725 with the U.S. Department of Energy. The United States Government retains and the publisher, by accepting the article for publication, acknowledges that the United States Government retains a non-exclusive, paid-up, irrevocable, world-wide license to publish or reproduce the published form of this manuscript, or allow others to do so, for United States Government purposes. The Department of Energy will provide public access to these results of federally sponsored research in accordance with the DOE Public Access Plan ( http://energy.gov/downloads/doe-public-access-plan ).

FundersFunder number
Battelle LLC
Carl ZeissNFE-19–07705
Oak Ridge National Laboratory
Office of Fusion Energy Sciences and Advanced Research Projects Agency- Energy
U.S. Department of Energy
Advanced Research Projects Agency - EnergyDE-AC05–00OR22725
Office of Energy Efficiency and Renewable Energy

    Keywords

    • Additive manufacturing
    • Crystallographic texture
    • Electron beam melting
    • Mechanical properties
    • Tungsten

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