Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel

D. T. Pierce; D. R. Coughlin; D. L. Williamson; K. D. Clarke; A. J. Clarke; J. G. Speer; D. K. Matlock; E. De Moor

Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel

D. T. Pierce, D. R. Coughlin, D. L. Williamson, K. D. Clarke, A. J. Clarke, J. G. Speer, D. K. Matlock, E. De Moor

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

7 Scopus citations

Abstract

Mossbauer effect spectroscopy (MES) and transmission electron microscopy (TEM) were used to study quenched and partitioned (Q&P) rmcrostructures in a 038C-l.54Mn-l.48Si wt. pet. (1.71C-1.52Mn-2.86Si at. pet.) steel, with an emphasis on characterizing transition carbides and retained austemte. Specimens were quenched to 225 or 250°C and partitioned at 400°C for times ranging from 10 to 300 s. The presence of n-carbides was confirmed by TEM and the quantities were measured by MES. The amounts of η-carbide ranged from 1.5 to 2.3 at. pet. and increased with partitioning time, accounting for a substantial portion (-27 to 41 pet.) of the total bulk carbon content of the steel. The amount (5.0 at. pet.) of η-carbide that formed after quenching and tempering (Q&T) at 400°C for 300 s was significantly greater than following partitioning at 400°C for 300 s (2.3 at. pet.), indicating that carbon partitioning from martensite to austemte competes with η-carbide formation dunng Q&P.

Original language	English
Title of host publication	PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015
Editors	Long-Qing Chen, Matthias Militzer, Gianluigi Botton, James Howe, Chadwick Sinclair, Hatem Zurob
Publisher	International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015
Pages	91-98
Number of pages	8
ISBN (Electronic)	9780692437360
State	Published - 2015
Externally published	Yes
Event	International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, PTM 2015 - Whistler, Canada Duration: Jun 28 2015 → Jul 3 2015

Publication series

Name	PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015

Conference

Conference	International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, PTM 2015
Country/Territory	Canada
City	Whistler
Period	06/28/15 → 07/3/15

Keywords

Mössbauer spectroscopy
Quenching and partitioning
Steel
Transition carbides

Cite this

Pierce, D. T., Coughlin, D. R., Williamson, D. L., Clarke, K. D., Clarke, A. J., Speer, J. G., Matlock, D. K., & De Moor, E. (2015). Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel. In L.-Q. Chen, M. Militzer, G. Botton, J. Howe, C. Sinclair, & H. Zurob (Eds.), PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015 (pp. 91-98). (PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015). International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015.

Pierce, D. T. ; Coughlin, D. R. ; Williamson, D. L. et al. / Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel. PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015. editor / Long-Qing Chen ; Matthias Militzer ; Gianluigi Botton ; James Howe ; Chadwick Sinclair ; Hatem Zurob. International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, 2015. pp. 91-98 (PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015).

@inproceedings{d621661b2b4c40e69b0d90c628790e04,

title = "M{\"o}ssbauer spectroscopy investigation of transition carbides in quenched and partitioned steel",

abstract = "Mossbauer effect spectroscopy (MES) and transmission electron microscopy (TEM) were used to study quenched and partitioned (Q&P) rmcrostructures in a 038C-l.54Mn-l.48Si wt. pet. (1.71C-1.52Mn-2.86Si at. pet.) steel, with an emphasis on characterizing transition carbides and retained austemte. Specimens were quenched to 225 or 250°C and partitioned at 400°C for times ranging from 10 to 300 s. The presence of n-carbides was confirmed by TEM and the quantities were measured by MES. The amounts of η-carbide ranged from 1.5 to 2.3 at. pet. and increased with partitioning time, accounting for a substantial portion (-27 to 41 pet.) of the total bulk carbon content of the steel. The amount (5.0 at. pet.) of η-carbide that formed after quenching and tempering (Q&T) at 400°C for 300 s was significantly greater than following partitioning at 400°C for 300 s (2.3 at. pet.), indicating that carbon partitioning from martensite to austemte competes with η-carbide formation dunng Q&P.",

keywords = "M{\"o}ssbauer spectroscopy, Quenching and partitioning, Steel, Transition carbides",

author = "Pierce, {D. T.} and Coughlin, {D. R.} and Williamson, {D. L.} and Clarke, {K. D.} and Clarke, {A. J.} and Speer, {J. G.} and Matlock, {D. K.} and {De Moor}, E.",

year = "2015",

language = "English",

series = "PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015",

publisher = "International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015",

pages = "91--98",

editor = "Long-Qing Chen and Matthias Militzer and Gianluigi Botton and James Howe and Chadwick Sinclair and Hatem Zurob",

booktitle = "PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015",

note = "International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, PTM 2015 ; Conference date: 28-06-2015 Through 03-07-2015",

}

Pierce, DT, Coughlin, DR, Williamson, DL, Clarke, KD, Clarke, AJ, Speer, JG, Matlock, DK & De Moor, E 2015, Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel. in L-Q Chen, M Militzer, G Botton, J Howe, C Sinclair & H Zurob (eds), PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015. PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, pp. 91-98, International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, PTM 2015, Whistler, Canada, 06/28/15.

Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel. / Pierce, D. T.; Coughlin, D. R.; Williamson, D. L. et al.
PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015. ed. / Long-Qing Chen; Matthias Militzer; Gianluigi Botton; James Howe; Chadwick Sinclair; Hatem Zurob. International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, 2015. p. 91-98 (PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel

AU - Pierce, D. T.

AU - Coughlin, D. R.

AU - Williamson, D. L.

AU - Clarke, K. D.

AU - Clarke, A. J.

AU - Speer, J. G.

AU - Matlock, D. K.

AU - De Moor, E.

PY - 2015

Y1 - 2015

N2 - Mossbauer effect spectroscopy (MES) and transmission electron microscopy (TEM) were used to study quenched and partitioned (Q&P) rmcrostructures in a 038C-l.54Mn-l.48Si wt. pet. (1.71C-1.52Mn-2.86Si at. pet.) steel, with an emphasis on characterizing transition carbides and retained austemte. Specimens were quenched to 225 or 250°C and partitioned at 400°C for times ranging from 10 to 300 s. The presence of n-carbides was confirmed by TEM and the quantities were measured by MES. The amounts of η-carbide ranged from 1.5 to 2.3 at. pet. and increased with partitioning time, accounting for a substantial portion (-27 to 41 pet.) of the total bulk carbon content of the steel. The amount (5.0 at. pet.) of η-carbide that formed after quenching and tempering (Q&T) at 400°C for 300 s was significantly greater than following partitioning at 400°C for 300 s (2.3 at. pet.), indicating that carbon partitioning from martensite to austemte competes with η-carbide formation dunng Q&P.

AB - Mossbauer effect spectroscopy (MES) and transmission electron microscopy (TEM) were used to study quenched and partitioned (Q&P) rmcrostructures in a 038C-l.54Mn-l.48Si wt. pet. (1.71C-1.52Mn-2.86Si at. pet.) steel, with an emphasis on characterizing transition carbides and retained austemte. Specimens were quenched to 225 or 250°C and partitioned at 400°C for times ranging from 10 to 300 s. The presence of n-carbides was confirmed by TEM and the quantities were measured by MES. The amounts of η-carbide ranged from 1.5 to 2.3 at. pet. and increased with partitioning time, accounting for a substantial portion (-27 to 41 pet.) of the total bulk carbon content of the steel. The amount (5.0 at. pet.) of η-carbide that formed after quenching and tempering (Q&T) at 400°C for 300 s was significantly greater than following partitioning at 400°C for 300 s (2.3 at. pet.), indicating that carbon partitioning from martensite to austemte competes with η-carbide formation dunng Q&P.

KW - Mössbauer spectroscopy

KW - Quenching and partitioning

KW - Steel

KW - Transition carbides

UR - http://www.scopus.com/inward/record.url?scp=84962630160&partnerID=8YFLogxK

M3 - Conference contribution

AN - SCOPUS:84962630160

T3 - PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015

SP - 91

EP - 98

BT - PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015

A2 - Chen, Long-Qing

A2 - Militzer, Matthias

A2 - Botton, Gianluigi

A2 - Howe, James

A2 - Sinclair, Chadwick

A2 - Zurob, Hatem

PB - International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015

T2 - International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015, PTM 2015

Y2 - 28 June 2015 through 3 July 2015

ER -

Pierce DT, Coughlin DR, Williamson DL, Clarke KD, Clarke AJ, Speer JG et al. Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel. In Chen LQ, Militzer M, Botton G, Howe J, Sinclair C, Zurob H, editors, PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015. International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015. 2015. p. 91-98. (PTM 2015 - Proceedings of the International Conference on Solid-Solid Phase Transformations in Inorganic Materials 2015).

Mössbauer spectroscopy investigation of transition carbides in quenched and partitioned steel

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