Joining of β-SiC by spark plasma sintering

Salvatore Grasso, Peter Tatarko, Stefano Rizzo, Harshit Porwal, Chunfeng Hu, Yutai Katoh, Milena Salvo, Michael J. Reece, Monica Ferraris

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101 Scopus citations

Abstract

Spark plasma sintering (SPS) was employed to join monolithic β-SiC with or without titanium as intermediate joining material. Both the localized and rapid heating contributed to the inherent energy saving of electric current assisted joining technique. The effects of uniaxial pressure and surface preparation were analyzed independently with respect to the flexural strength and the morphology of the joints. In particular samples polished down to 1. μm and joined at 1900. °C for 5. min achieved the strength of the as received material. The failure occurred outside the joining interface, confirming the optimum quality of the joint. Pressure in combination with surface preparation was necessary to achieve perfect adhesion and pore free direct joining of SiC. The use of Ti foil as a joining material and pressure allowed joining of unpolished SiC.

Original languageEnglish
Pages (from-to)1681-1686
Number of pages6
JournalJournal of the European Ceramic Society
Volume34
Issue number7
DOIs
StatePublished - Jul 2014

Funding

The research leading to these results was supported by the European Union's Seventh Framework Programme managed by REA-Research Executive Agency ( http://www.ec.europa.eu/research/rea ) (Marie Curie Action, GlaCERCo GA 264526).

Keywords

  • Joining
  • Spark plasma sintering
  • β-SiC

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