Investigating the failure behavior of cast Al-11Ce-0.4Mg alloys using in-situ scanning electron microscopy tensile testing

Ryan J. Lane, Michael S. Kesler, Kashif Nawaz, Reza Mirzaeifar

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4 Scopus citations

Abstract

Within the last decade, research on Al-Ce-Mg alloys has reported promising results for use in cast part applications. In this paper, the failure behavior of cast Al-11Ce-0.4Mg (wt%) was investigated experimentally with focus on the effect the matrix and intermetallic phases have on the fracture propagation behavior at failure. For the first time, in-situ SEM tensile testing was used to study the failure behavior of cast Al-Ce alloys, reporting results for uniaxial, DIC, and single edge notch tensile tests. The results of the in-situ SEM tensile testing were compared with the materials characterization experiments, which included serial sectioning, EBSD, EDS, and fractography. Analysis of EBSD and EDS mapping of cast Al-11Ce-0.4Mg showed that the cast microstructure was a hypereutectic two phase Al-Ce alloy with grains encompassing large complex colonies of laminar eutectic Al11Ce3 intermetallic. The uniaxial tensile results reported the effect casting defects have on the strength and ductility of the alloy, and DIC in-situ testing showed that the eutectic colonies plastically deform less than the matrix phase. In-situ SEM single edge notch tensile testing displayed how the strength of an individual phase affected the crack propagation direction in the alloy. The results of both the materials characterization and in-situ tensile testing experiments on the failure of this alloy revealed further directions for future alloy development that can improve both the strength and fracture toughness of Al-Ce-Mg alloys.

Original languageEnglish
Article number169491
JournalJournal of Alloys and Compounds
Volume947
DOIs
StatePublished - Jun 25 2023

Funding

This work was sponsored by the US Department of Energy Building Technologies Office under Contract No. 0008-1534 (BTO Lab Call 2021) and NFE-17-06541 with UT-Battele, LLC. We would also like to thank the Critical Materials Institute, an Energy Innovation Hub funded by the U.S. Department of Energy, and Eck Industries for providing material samples. This work used shared facilities at the Virginia Tech Nanoscale Characterization and Fabrication Laboratory (NCFL) part of the National Center for Earth and Environmental Nanotechnology Infrastructure (NanoEarth), a member of the National Nanotechnology Coordinated Infrastructure (NNCI), supported by NSF ( ECCS 1542100 and ECCS 2025151 ). Finally, the authors would like to give a special thank you to Professor John C. Duke of the Engineering Mechanics Department at Virginia Tech for his insight and suggestions during editing of this manuscript.

FundersFunder number
Critical Materials Institute
National Center for Earth and Environmental Nanotechnology Infrastructure
National Science FoundationECCS 1542100, ECCS 2025151
U.S. Department of Energy
Building Technologies OfficeNFE-17-06541, 0008-1534
Eck Industries

    Keywords

    • Aluminum cerium alloys (Al-Ce)
    • Failure behavior
    • Tensile in-situ scanning electron microscopy testing

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