Abstract
Deformation twinning plays a critical role on improving metals or alloys ductility, especially for hexagonal close-packed materials with low symmetry crystal structure. A rolled Mg alloy was selected as a model system to investigate the extension twinning behaviors and characteristics of parent-twin interactions by nondestructive in situ 3D synchrotron X-ray microbeam diffraction. Besides twinning-detwinning process, the “twinning-like” lattice reorientation process was captured within an individual grain inside a bulk material during the strain reversal. The distributions of parent, twin, and reorientated grains and sub-micron level strain variation across the twin boundary are revealed. A theoretical calculation of the lattice strain confirms that the internal strain distribution in parent and twinned grains correlates with the experimental setup, grain orientation of parent, twin, and surrounding grains, as well as the strain path changes. The study suggests a novel deformation mechanism within the hexagonal close-packed structure that cannot be determined from surface-based characterization methods.
Original language | English |
---|---|
Pages (from-to) | 15-23 |
Number of pages | 9 |
Journal | Acta Materialia |
Volume | 121 |
DOIs | |
State | Published - Dec 1 2016 |
Bibliographical note
Publisher Copyright:© 2016 Acta Materialia Inc.
Funding
This manuscript has been authored by UT-Battelle, LLC under Contract No. DE-AC05-00OR22725 with the U.S. Department of Energy. The United States Government retains and the publisher, by accepting the article for publication, acknowledges that the United States Government retains a non-exclusive, paid-up, irrevocable, world-wide license to publish or reproduce the published form of this manuscript, or allow others to do so, for United States Government purposes. The Department of Energy will provide public access to these results of federally sponsored research in accordance with the DOE Public Access Plan ( http://energy.gov/downloads/doe-public-access-plan ). The synchrotron X-ray, neutron and EBSD works were carried out at the Advanced Photon Source (APS), Argonne National Laboratory (ANL), Spallation Neutron Source (SNS), Oak Ridge National Laboratory (ORNL), and Center for Nanophase Materials Sciences, ORNL, respectively, supported by the U.S. Department of Energy, Basic Energy Sciences, Scientific User Facilities Division. W.W. is supported by a Laboratory Directed Research and Development (LDRD) project ( LDRD-6789 ) of ORNL. Y.F.G. acknowledges support from National Science Foundation CMMI 1300223 . P.K.L. would like to acknowledge the Department of Energy (DOE), Office of Fossil Energy , National Energy Technology Laboratory ( DE-FE-0008855 and DE-FE-0024054 , and DE-FE-0011194 ), with Mr. V. Cedro and Mr. R. Dunst as program managers. P.K.L. thanks the support from the project of DE-FE-0011194 with the program manager, Dr. J. Mullen. P.K.L. thanks the support from the National Science Foundation CMMI-1100080.
Funders | Funder number |
---|---|
Center for Nanophase Materials Sciences | |
National Science Foundation | CMMI 1300223 |
U.S. Department of Energy | |
Office of Fossil Energy | |
Basic Energy Sciences | |
Argonne National Laboratory | |
Oak Ridge National Laboratory | |
Laboratory Directed Research and Development | LDRD-6789 |
National Energy Technology Laboratory | CMMI-1100080, DE-FE-0024054, DE-FE-0011194, DE-FE-0008855 |
Keywords
- Deformation mechanism
- Magnesium alloy
- Synchrotron X-ray
- Twinning