Abstract
Ti–6Al–4V parts fabricated via electron beam melting (EBM) powder bed fusion are often subjected to hot isostatic pressing below the β-transus temperature to mitigate defects. During which the pressure aids in pore closure and the thermal exposure results in coarsening of α phase while retaining the columnar prior-β phase grain morphology present in the as-fabricated condition. The same post-processing treatment can also be carried out above β-transus temperature which is an effective way to modify both the grain morphology and the associated α textures. The objective of this work is to correlate thermally induced microstructural changes to the deformation and fracture response of the EBM processed Ti–6Al–4V. To this end, we have carried out both sub-transus and super-transus heat-treatments of the as-fabricated material. The mechanical response of the as-fabricated and all heat-treated materials are characterized by in-situ tensile tests under a high-resolution digital optical microscope. This enabled us to capture large-scale panoramic images of the deforming microstructure, and overcome the trade-off between the image resolution and the field of view during in-situ experiments. The series of images captured throughout the imposed deformation are subsequently used to perform microstructure-based digital image correlation to measure microstructural-scale strains over a large area. The results of the in-situ tests together with detailed fractographic analyses are then used to elucidate how the heterogeneous deformation spanning over multiple microstructural length-scales, for example, at the scale of lamellae, colonies of lamellae and grain boundaries, affect the overall deformation and fracture response of the post-processed materials.
Original language | English |
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Article number | 139986 |
Journal | Materials Science and Engineering: A |
Volume | 795 |
DOIs | |
State | Published - Sep 23 2020 |
Funding
The samples were fabricated at the U.S. Department of Energy's Manufacturing Demonstration Facility, located at Oak Ridge National Laboratory. PN gratefully acknowledges the financial support provided by the U.S. Department of Energy, Office of Energy Efficiency and Renewable Energy, Advanced Manufacturing Office , under Contract DE-AC05-00OR22725 with UT-Battelle, LLC. AS gratefully acknowledges the financial support provided by the US Army Research Laboratory through the cooperative agreement – Materials and Manufacturing Processes for the Army of the Future and the Haythornthwaite Foundation through the ASME/AMD – Haythornthwaite Research Initiation Grant. The samples were fabricated at the U.S. Department of Energy's Manufacturing Demonstration Facility, located at Oak Ridge National Laboratory. PN gratefully acknowledges the financial support provided by the U.S. Department of Energy, Office of Energy Efficiency and Renewable Energy, Advanced Manufacturing Office, under Contract DE-AC05-00OR22725 with UT-Battelle, LLC. AS gratefully acknowledges the financial support provided by the US Army Research Laboratory through the cooperative agreement ? Materials and Manufacturing Processes for the Army of the Future and the Haythornthwaite Foundation through the ASME/AMD ? Haythornthwaite Research Initiation Grant.
Funders | Funder number |
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Haythornthwaite Foundation | |
U.S. Department of Energy | |
Advanced Micro Devices | |
Advanced Manufacturing Office | DE-AC05-00OR22725 |
Office of Energy Efficiency and Renewable Energy | |
Oak Ridge National Laboratory | |
Army Research Laboratory | |
American Society of Mechanical Engineers |
Keywords
- Additive manufacturing
- Characterization
- Digital image correlation
- Fracture behavior
- In situ tension test
- Titanium alloys