Identifying the effect of coherent precipitates on the deformation mechanisms by in situ neutron diffraction in an extruded magnesium alloy under low-cycle fatigue conditions

As a new class of heat-treatable magnesium alloys, the low-alloyed Mg-Al-Ca-Mn alloy has great engineering potential because of its excellent extrudability and high strength by the dispersion of Guinier-Preston (G.P.) zones. The complex deformation mechanisms associated with hexagonal crystals, the interactions between defects with such G.P. zones, as well as their impacts on fatigue lifetime, are all critical issues before the actual deployment of such materials. In this study, this type of Mg alloy with and without G.P. zone dispersion during cyclic deformation was investigated by in situ neutron diffraction measurements. The relationship between the macroscopic cyclic deformation behavior and the microscopic response (particularly twinning and detwinning) at the grain level was established. The general deformation mechanism evolution in samples under the solution-treated (S.T.) state was generally similar to that in samples under the peak-aged (P.A.) state. Both samples plastically deformed by extension twinning during compression, and by a sequential process of detwinning and dislocation motion under reverse tension. Results suggest that the precipitates provided the greatest strengthening against the prismatic slip (∼ 45% increase), the moderate to the {101¯2} extension twinning (∼ 27 %), and the least to the basal slip (∼ 11% increase). The P.A. samples have shorter fatigue lifetime primarily due to the excessive dislocation pileups and the higher backstress that promote crack initiation.