High spatial resolution x-ray microanalysis of radiation-induced segregation in proton-irradiated stainless steels

E. A. Kenik, J. T. Busby, G. S. Was

Research output: Contribution to journalArticlepeer-review

Abstract

The spatial redistribution of alloying elements and impurities near grain boundaries in several stainless steel alloys arising from non-equilibrium processes have been measured by analytical electron microscopy (AEM) in a field emission scanning transmission electron microscope. Radiation-induced segregation (RIS) has been shown to result in significant compositional changes at point defects sinks, such as grain boundaries. The influence of irradiation dose and temperature, alloy composition, prior heat treatment, and post-irradiation annealing on the grain boundary composition profiles have been investigated. Understanding the importance of these microchemical changes relative to the radiation-induced microstructural change in irradiation-assisted stress corrosion cracking (IASCC) of the irradiated materials is the primary goal of this study.

Original languageEnglish
Pages (from-to)295-300
Number of pages6
JournalMaterials Research Society Symposium - Proceedings
Volume589
StatePublished - 2000
Externally publishedYes

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