High Resolution Neutron Radiography and Tomography of Hydrided Zircaloy-4 Cladding Materials

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Abstract

Hydrogen content and distribution in Zircaloy-4 cladding samples with controlled hydrogen concentrations up to 1100 ppm were studied using neutron radiography and computed tomography. Hydrogen charging was performed in a process tube that was heated to facilitate hydrogen absorption by the metal. A correlation between the hydrogen concentration in the hydrided tubes and the neutron intensity was established, by which hydrogen content can be determined precisely in a small area (55 μm × 55 μm). Image analysis was also performed to evaluate the heating rate and its correlation with the hydrogen distribution through hydrided materials. In addition to image analysis, tomography experiments were performed on Zircaloy-4 tube samples to study the local hydrogen distribution. A 3D reconstruction of the tube was evaluated in which an uneven hydrogen distribution in the circumferential direction can be observed.

Original languageEnglish
Pages (from-to)478-482
Number of pages5
JournalPhysics Procedia
Volume69
DOIs
StatePublished - 2015
EventProceedings of the 10th World Conference on Neutron Radiography, WCNR-10 2014 - Grindelwald, Switzerland
Duration: Oct 5 2014Oct 10 2014

Funding

This research was sponsored by the Laboratory Directed Research and Development Program of Oak Ridge National Laboratory, managed by UT-Battelle, LLC, for the U.S. Department of Energy under Contract No. DE-AC05-00OR22725. This research was performed at Oak Ridge National Laboratory's High Flux Isotope Reactor, which is sponsored by the Scientific User Facilities Division, Office of Basic Energy Sciences, U. S. DOE, which is managed by UT-Battelle, LLC.

FundersFunder number
Oak Ridge National Laboratory
Office of Basic Energy Sciences
Scientific User Facilities Division
U. S. DOE
U.S. Department of Energy
Oak Ridge National Laboratory

    Keywords

    • Zirconum
    • hydride
    • hydrogen distribution
    • neutron radiography
    • neutron tomography

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