TY - JOUR
T1 - Glycine-nitrate synthesis of Sr doped La2Zr2O 7 pyrochlore powder
AU - Orlovskaya, N.
AU - Chen, Y.
AU - Miller, N.
AU - Abernathy, H.
AU - Haynes, D.
AU - Tucker, D.
AU - Gemmen, R.
PY - 2011/1/1
Y1 - 2011/1/1
N2 - Materials with A2B2O7 (pyrochlore) structure have received significant attention for their applications as new protonic conductors and materials used in electronic devices. One of the unique synthesis routes for La2Zr2O7 (pyrochlore) powders is the glycine-nitrate combustion method, which shows superior properties of the synthesised powder using glycine as a complexing agent. The Sr doped La2Zr2O7 powders in pure pyrochlore structure were produced using this approach. Selected characteristics of the synthesised powders, such as crystal structure, lattice parameters, crystallite size, the vibrational properties, the morphology of the particles, along with the specific surface area and particle size, have been investigated. The dependence of some properties on annealing temperatures of the powders has been studied.
AB - Materials with A2B2O7 (pyrochlore) structure have received significant attention for their applications as new protonic conductors and materials used in electronic devices. One of the unique synthesis routes for La2Zr2O7 (pyrochlore) powders is the glycine-nitrate combustion method, which shows superior properties of the synthesised powder using glycine as a complexing agent. The Sr doped La2Zr2O7 powders in pure pyrochlore structure were produced using this approach. Selected characteristics of the synthesised powders, such as crystal structure, lattice parameters, crystallite size, the vibrational properties, the morphology of the particles, along with the specific surface area and particle size, have been investigated. The dependence of some properties on annealing temperatures of the powders has been studied.
KW - Glycine-nitrate synthesis
KW - LaZrO
KW - Powders
KW - Pyrochlore
UR - http://www.scopus.com/inward/record.url?scp=78651094463&partnerID=8YFLogxK
U2 - 10.1179/174367510X12753884125569
DO - 10.1179/174367510X12753884125569
M3 - Article
AN - SCOPUS:78651094463
SN - 1743-6753
VL - 110
SP - 54
EP - 57
JO - Advances in Applied Ceramics
JF - Advances in Applied Ceramics
IS - 1
ER -