Abstract
Microstructural variation of additively manufactured (AM) metal components in comparison to wrought counterparts makes certification for critical applications a challenge. Microscale simulations leveraging modern computational tools may be used to supplement testing of AM microstructures, thus accelerating certification by reducing the number of experiments needed. However, as micromechanical response is closely tied to critical properties like fatigue-life and fracture, utilization of these simulations with macroscale experimental data alone is insufficient. One means to attain microscale experimental data is in situ diffraction data collected from synchrotron X-ray sources. In this work, such data were collected during in situ compression of AM Inconel 625 superalloy. Interpretation of experimental results was assisted by massive (8M element) complementary micromechanical simulations performed on sets of virtual microstructures generated using cellular automata. Together, micromechanical data from diffraction experiments and simulations were used to probe the effects of textured “track” microstructures generated during laser powder bed fusion and directional strength-to-stiffness on micromechanical response. Though fiber-averaged directional strength-to-stiffness ratios were expected to dominate given the high elastic anisotropy of the material, the combination of small variations in texture and specific grain configurations unique to AM microstructures lead to significant variability in micromechanical response after yield. The findings emphasize the importance of high-fidelity microstructural representation that captures key texture components and AM-specific morphology for property prediction of AM metals.
| Original language | English |
|---|---|
| Article number | 148824 |
| Journal | Materials Science and Engineering: A |
| Volume | 944 |
| DOIs | |
| State | Published - Nov 2025 |
Funding
We thank Dr. Lyle Levine (NIST) for providing the bridge specimen from which the compression specimens were extracted. We also thank Dr. Alyssa Maich (LLNL) for collecting the EBSD data presented in Section 2. RJK and DCP acknowledge support from LLNL Contract #B652591. This work is based on research conducted at the Center for High-Energy X-ray Sciences (CHEXS) at CHESS, which is supported by the National Science Foundation (BIO, ENG, and MPS Directorates) under award DMR-1829070. This research was supported by the Exascale Computing Project (17-SC-20-SC), a collaborative effort of the U.S. DOE Office of Science and the NNSA. This work was performed under the auspices of the U.S. Department of Energy by Lawrence Livermore National Laboratory under Contract DE-AC52-07NA27344. This manuscript has been in part authored by UT-Battelle, LLC, under contract DE-AC05-00OR22725 with the US Department of Energy (DOE). The US government retains and the publisher, by accepting the article for publication, acknowledges that the US government retains a nonexclusive, paid-up, irrevocable, worldwide license to publish or reproduce the published form of this manuscript, or allow others to do so, for US government purposes. DOE will provide public access to these results of federally sponsored research in accordance with the DOE Public Access Plan (https://www.energy.gov/doe-public-access-plan).
Keywords
- Additive manufacturing
- Crystal plasticity
- Nickel superalloy
- X-ray diffraction