Development of a complex multicomponent microstructure on commercial carbon-silicon grade steel by governing the phase transformation mechanisms to design novel quenching and partitioning processing

Felipe M. Carvalho, Dany Centeno, Gustavo Tressia, Julian A. Avila, Fabiano E.M. Cezario, Andrés Márquez-Rossy, Edwan A. Ariza, Mohammad Masoumi

Research output: Contribution to journalArticlepeer-review

15 Scopus citations

Abstract

The constant demand for increasing the strength without ductility loss and production cost encourages industrial and academic societies to propose novel heat treatment processing of commercial steel grades. To improve the mechanical properties of commercial spring steel, a novel quenching and partitioning (Q&P) processing was designed to deliver a complex and desirable nanostructured multicomponent microstructure by controlling the carbon partitioning kinetics. Furthermore, the partitioning of excessive carbon from saturated martensite into untransformed austenite enhances the formation of transition carbides during tempering between 130 and 280 °C. Electron microscopy confirmed a complex multicomponent structure containing BCC tempered lath combined with retained austenite and nanocarbides particles within the tempered laths. Such multicomponent lath-type structure obtained by designed Q&P heat treatment on commercial carbon-silicon spring steel revealed localized mechanical resistance varying from 4.92 GPa for the QP-220-375-400 to 8.22 GPa for the QP-220-325-400 samples determined by nanoindentation test. Moreover, the tensile test showed high ultimate tensile strength and a yield strength up to 1400 MPa and 975 MPa, respectively, in the QP-220-375-400 sample due to a set of complex multicomponent lath-type refined structures designed by Q&P coupled with bainitic transformation, with good strain to fracture (∼0.12%).

Original languageEnglish
Pages (from-to)4590-4603
Number of pages14
JournalJournal of Materials Research and Technology
Volume18
DOIs
StatePublished - May 2022

Funding

The authors acknowledge the financial support provided by the National Council of Scientific and Technological Development - CNPq (grant number 304157/2020–1 and 309160/2016–2 ) and São Paulo Research Foundation – FAPESP (grant number 2021/02926–4 ). Julian A. Avila is a Serra Hunter Fellow.

Keywords

  • Boundaries
  • Crystal orientation
  • Kernel average misorientation
  • Lattice distortion
  • Nanoparticles

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