Deuterium incorporation in biomass cell wall components by NMR analysis

Marcus B. Foston; Joseph McGaughey; Hugh O'Neill; Barbara R. Evans; Arthur Ragauskas

doi:10.1039/c2an16025k

Deuterium incorporation in biomass cell wall components by NMR analysis

Marcus B. Foston, Joseph McGaughey, Hugh O'Neill, Barbara R. Evans, Arthur Ragauskas

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19 Scopus citations

Abstract

A commercially available deuterated kale sample was analyzed for deuterium incorporation by ionic liquid solution ²H and ¹H nuclear magnetic resonance (NMR). This protocol was found to effectively measure the percent deuterium incorporation at 33%, comparable to the 31% value determined by combustion. The solution NMR technique also suggested by a qualitative analysis that deuterium is preferentially incorporated into the carbohydrate components of the kale sample.

Original language	English
Pages (from-to)	1090-1093
Number of pages	4
Journal	Analyst
Volume	137
Issue number	5
DOIs	https://doi.org/10.1039/c2an16025k
State	Published - Mar 7 2012

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title = "Deuterium incorporation in biomass cell wall components by NMR analysis",

abstract = "A commercially available deuterated kale sample was analyzed for deuterium incorporation by ionic liquid solution 2H and 1H nuclear magnetic resonance (NMR). This protocol was found to effectively measure the percent deuterium incorporation at 33%, comparable to the 31% value determined by combustion. The solution NMR technique also suggested by a qualitative analysis that deuterium is preferentially incorporated into the carbohydrate components of the kale sample.",

author = "Foston, {Marcus B.} and Joseph McGaughey and Hugh O'Neill and Evans, {Barbara R.} and Arthur Ragauskas",

year = "2012",

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AU - Foston, Marcus B.

AU - McGaughey, Joseph

AU - O'Neill, Hugh

AU - Evans, Barbara R.

AU - Ragauskas, Arthur

PY - 2012/3/7

Y1 - 2012/3/7

N2 - A commercially available deuterated kale sample was analyzed for deuterium incorporation by ionic liquid solution 2H and 1H nuclear magnetic resonance (NMR). This protocol was found to effectively measure the percent deuterium incorporation at 33%, comparable to the 31% value determined by combustion. The solution NMR technique also suggested by a qualitative analysis that deuterium is preferentially incorporated into the carbohydrate components of the kale sample.

AB - A commercially available deuterated kale sample was analyzed for deuterium incorporation by ionic liquid solution 2H and 1H nuclear magnetic resonance (NMR). This protocol was found to effectively measure the percent deuterium incorporation at 33%, comparable to the 31% value determined by combustion. The solution NMR technique also suggested by a qualitative analysis that deuterium is preferentially incorporated into the carbohydrate components of the kale sample.

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U2 - 10.1039/c2an16025k

DO - 10.1039/c2an16025k

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VL - 137

SP - 1090

EP - 1093

JO - Analyst

JF - Analyst

IS - 5

ER -

Deuterium incorporation in biomass cell wall components by NMR analysis

Abstract

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