Defects and 3D structural inhomogeneity in electron beam additively manufactured Inconel 718

Andrew T. Polonsky, McLean P. Echlin, William C. Lenthe, Ryan R. Dehoff, Michael M. Kirka, Tresa M. Pollock

Research output: Contribution to journalArticlepeer-review

80 Scopus citations

Abstract

Material structure and defects created during additive manufacturing contribute to the variability in mechanical properties of these parts, limiting their use for critical applications. Three-dimensional crystallographic, structural, and chemical information in electron beam melted Inconel 718 was collected from the sub-micron to the millimeter scale using the TriBeam tomography system. The relationship of defects to the surrounding microstructure has been studied in detail. Lack of fusion defects created sharp discontinuities in the grain morphology that extended several build layers beyond the layer where the defect originated. Nitrides and carbides in the size range of 1.25 μm to 10 μm were observed throughout the volume, with pronounced nitride clustering. The similarities between solidification in additive manufacturing and traditional manufacturing processes are demonstrated by the comparable size and distribution of carbides measured for industrial-scale samples of 718. Defects created during additive manufacturing cannot be easily remedied via standard post-processing techniques, and will likely diminish the mechanical performance of additively manufactured parts.

Original languageEnglish
Pages (from-to)171-181
Number of pages11
JournalMaterials Characterization
Volume143
DOIs
StatePublished - Sep 2018

Funding

This work was supported by the DOE ’s Manufacturing Demonstration Facility (MDF) at ORNL through the RAMP-UP program (Award Number 4000145177 ). Additionally, this research was sponsored by the US Department of Energy, Office of Energy Efficiency and Renewable Energy, Advanced Manufacturing Office , under contract DE-AC05-00OR22725 with UT-Battelle, LLC. This work was supported by the DOE's Manufacturing Demonstration Facility (MDF) at ORNL through the RAMP-UP program (Award Number 4000145177). Additionally, this research was sponsored by the US Department of Energy, Office of Energy Efficiency and Renewable Energy, Advanced Manufacturing Office, under contract DE-AC05-00OR22725 with UT-Battelle, LLC.

FundersFunder number
DOE ’s Manufacturing Demonstration Facility
DOE's Manufacturing Demonstration Facility
U.S. Department of Energy
Myotonic Dystrophy Foundation
Advanced Manufacturing OfficeDE-AC05-00OR22725
Office of Energy Efficiency and Renewable Energy
Oak Ridge National Laboratory4000145177

    Keywords

    • Additive manufacturing
    • Electron beam melting
    • Lack of fusion
    • Microstructure
    • Tomography

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