Compact, portable, automatic sample changer stick for cryostats and closed-cycle refrigerators

Daniel Vong, Eric C. Novak, Mariano M. Ruiz-Rodriguez, Saad R. Elorfi, Benjamin Thomas, Amanda J. Morris, Adam J. Moulé, Luke L. Daemen

Research output: Contribution to journalArticlepeer-review

1 Scopus citations

Abstract

Beamlines are facilities that produce and deliver highly focused and intense beams of radiation, typically x rays, synchrotron radiation, or neutrons, for scientific research purposes. Millions of dollars are spent annually to maintain and operate these scientific beamlines, oftentimes running continuously between cycles. To reduce human intervention and improve productivity, mechanical sample changers are often commissioned for use. Designing sample changers is difficult because mechanical parts can be bulky, expensive, and challenging to design for instruments with low volume access, high radiation, and cryogenic environments. We present a portable and inexpensive sample changer stick that can hold and manipulate up to four samples, specifically designed for use with cryogenic closed-cycle refrigerators. The sample changer stick enables rapid and efficient exchange of samples without manual intervention, and is compatible with standard sample mounts such as vanadium cans. The sample changer stick includes a motorized rotation and lancing mechanism, which enables the precise positioning of each sample in the neutron beam, while ensuring compatibility with the operating temperatures and vacuum conditions required for closed-cycle refrigerators. The design has been successfully tested at the VISION beamline at the Spallation Neutron Source. The mechanical action and software controls are detailed. The sample changer stick is a valuable tool for scientists working with cryogenic closed-cycle refrigerators.

Original languageEnglish
Article number085108
JournalReview of Scientific Instruments
Volume94
Issue number8
DOIs
StatePublished - Aug 1 2023

Funding

This research was supported by the Department of Energy, Basic Energy Sciences, Award No. DE-SC0010419, including salary for D.V. and A.J.M. from UC Davis. This research uses the resources at the Spallation Neutron Source, a DOE Office of Science user facility operated by the Oak Ridge National Laboratory, partly supported by LLNL under Contract No. DE-AC52-07NA27344. Samples were prepared by B.T. and A.J.M. from Virginia-Tech and supported under Department of Energy Grant No. DE-SC0012445. This material is based upon the work supported by the U.S. Department of Energy, Office of Science, Office of Workforce Development for Teachers and Scientists, Office of Science Graduate Student Research (SCGSR) program. The SCGSR program is administered by the Oak Ridge Institute for Science and Education (ORISE) for the DOE. ORISE is managed by ORAU under Contract No. DE-SC0014664. All opinions expressed in this paper are the author’s and do not necessarily reflect the policies and views of DOE, ORAU, or ORISE.

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