Chromatographic determination of the phosphate anions in crystalline and glassy Na4NbP3Oz

B. C. Sales; B. C. Chakoumakos

doi:10.1006/jssc.1993.1232

Chromatographic determination of the phosphate anions in crystalline and glassy Na₄NbP₃O_z

B. C. Sales, B. C. Chakoumakos

Single Crystal Diffraction

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Abstract

High-performance liquid chromatography (HPLC) measurements on crystalline and glassy Na₄NbP₃O_z prove that the crystalline phase is a pyrophosphate and that the glassy material contains a distribution of phosphate anions with anions up to five PO₄ tetrahedra in length. Powder X-ray diffraction data for a new trimetaphosphate crystalline phase with the composition Na₃NbP₃O_x are also reported.

Original language	English
Pages (from-to)	406-409
Number of pages	4
Journal	Journal of Solid State Chemistry
Volume	105
Issue number	2
DOIs	https://doi.org/10.1006/jssc.1993.1232
State	Published - Aug 1993

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title = "Chromatographic determination of the phosphate anions in crystalline and glassy Na4NbP3Oz",

abstract = "High-performance liquid chromatography (HPLC) measurements on crystalline and glassy Na4NbP3Oz prove that the crystalline phase is a pyrophosphate and that the glassy material contains a distribution of phosphate anions with anions up to five PO4 tetrahedra in length. Powder X-ray diffraction data for a new trimetaphosphate crystalline phase with the composition Na3NbP3Ox are also reported.",

author = "Sales, {B. C.} and Chakoumakos, {B. C.}",

year = "1993",

month = aug,

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AU - Sales, B. C.

AU - Chakoumakos, B. C.

PY - 1993/8

Y1 - 1993/8

N2 - High-performance liquid chromatography (HPLC) measurements on crystalline and glassy Na4NbP3Oz prove that the crystalline phase is a pyrophosphate and that the glassy material contains a distribution of phosphate anions with anions up to five PO4 tetrahedra in length. Powder X-ray diffraction data for a new trimetaphosphate crystalline phase with the composition Na3NbP3Ox are also reported.

AB - High-performance liquid chromatography (HPLC) measurements on crystalline and glassy Na4NbP3Oz prove that the crystalline phase is a pyrophosphate and that the glassy material contains a distribution of phosphate anions with anions up to five PO4 tetrahedra in length. Powder X-ray diffraction data for a new trimetaphosphate crystalline phase with the composition Na3NbP3Ox are also reported.

UR - http://www.scopus.com/inward/record.url?scp=0006856395&partnerID=8YFLogxK

U2 - 10.1006/jssc.1993.1232

DO - 10.1006/jssc.1993.1232

M3 - Article

AN - SCOPUS:0006856395

SN - 0022-4596

VL - 105

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EP - 409

JO - Journal of Solid State Chemistry

JF - Journal of Solid State Chemistry

IS - 2

ER -

Chromatographic determination of the phosphate anions in crystalline and glassy Na₄NbP₃O_z

Abstract

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