Characterization of the oxidation-sulfidation of a preoxidized ODS FeCrAl alloy

B. A. Pint; B. M. Banks; J. C. Duncan; A. J. Garratt-Reed; L. W. Hobbs

Characterization of the oxidation-sulfidation of a preoxidized ODS FeCrAl alloy

B. A. Pint, B. M. Banks, J. C. Duncan, A. J. Garratt-Reed, L. W. Hobbs

Research output: Contribution to journal › Conference article › peer-review

3 Scopus citations

Abstract

In this study, preoxidations of a Y₂O₃-dispersed FeCrAlFi alloy (MA956) were done in 1atm of dry, flowing O₂ for 2hr at 1000°C. Weight gains were measured during oxidation using Cahn 1000 microbalance and after oxidation using a Mettler AE163 balance. SEM observations of the scale surface before and after exposure to the O-S environment indicated almost no change in the scale surface morphology. TEM samples were made parallel to the sample surface near the oxide-gas interface and near the metal-oxide interface to study the possible penetration of sulfur into the preoxidized scale by cracks or grain boundaries. The samples were analyzed in a FEG-STEM equipped with XEDS.

Original language	English
Pages (from-to)	1146-1147
Number of pages	2
Journal	Proceedings - Annual Meeting, Microscopy Society of America
State	Published - 1993
Externally published	Yes
Event	Proceedings of the 51st Annual Meeting Microscopy Society of America - Cincinnati, OH, USA Duration: Aug 1 1993 → Aug 6 1993

Cite this

@article{d59612a1952e4fe29e998ca586882192,

title = "Characterization of the oxidation-sulfidation of a preoxidized ODS FeCrAl alloy",

abstract = "In this study, preoxidations of a Y2O3-dispersed FeCrAlFi alloy (MA956) were done in 1atm of dry, flowing O2 for 2hr at 1000°C. Weight gains were measured during oxidation using Cahn 1000 microbalance and after oxidation using a Mettler AE163 balance. SEM observations of the scale surface before and after exposure to the O-S environment indicated almost no change in the scale surface morphology. TEM samples were made parallel to the sample surface near the oxide-gas interface and near the metal-oxide interface to study the possible penetration of sulfur into the preoxidized scale by cracks or grain boundaries. The samples were analyzed in a FEG-STEM equipped with XEDS.",

author = "Pint, \{B. A.\} and Banks, \{B. M.\} and Duncan, \{J. C.\} and Garratt-Reed, \{A. J.\} and Hobbs, \{L. W.\}",

year = "1993",

language = "English",

pages = "1146--1147",

journal = "Proceedings - Annual Meeting, Microscopy Society of America",

issn = "0424-8201",

note = "Proceedings of the 51st Annual Meeting Microscopy Society of America ; Conference date: 01-08-1993 Through 06-08-1993",

}

TY - JOUR

T1 - Characterization of the oxidation-sulfidation of a preoxidized ODS FeCrAl alloy

AU - Pint, B. A.

AU - Banks, B. M.

AU - Duncan, J. C.

AU - Garratt-Reed, A. J.

AU - Hobbs, L. W.

PY - 1993

Y1 - 1993

N2 - In this study, preoxidations of a Y2O3-dispersed FeCrAlFi alloy (MA956) were done in 1atm of dry, flowing O2 for 2hr at 1000°C. Weight gains were measured during oxidation using Cahn 1000 microbalance and after oxidation using a Mettler AE163 balance. SEM observations of the scale surface before and after exposure to the O-S environment indicated almost no change in the scale surface morphology. TEM samples were made parallel to the sample surface near the oxide-gas interface and near the metal-oxide interface to study the possible penetration of sulfur into the preoxidized scale by cracks or grain boundaries. The samples were analyzed in a FEG-STEM equipped with XEDS.

AB - In this study, preoxidations of a Y2O3-dispersed FeCrAlFi alloy (MA956) were done in 1atm of dry, flowing O2 for 2hr at 1000°C. Weight gains were measured during oxidation using Cahn 1000 microbalance and after oxidation using a Mettler AE163 balance. SEM observations of the scale surface before and after exposure to the O-S environment indicated almost no change in the scale surface morphology. TEM samples were made parallel to the sample surface near the oxide-gas interface and near the metal-oxide interface to study the possible penetration of sulfur into the preoxidized scale by cracks or grain boundaries. The samples were analyzed in a FEG-STEM equipped with XEDS.

UR - https://www.scopus.com/pages/publications/0027704940

M3 - Conference article

AN - SCOPUS:0027704940

SN - 0424-8201

SP - 1146

EP - 1147

JO - Proceedings - Annual Meeting, Microscopy Society of America

JF - Proceedings - Annual Meeting, Microscopy Society of America

T2 - Proceedings of the 51st Annual Meeting Microscopy Society of America

Y2 - 1 August 1993 through 6 August 1993

ER -

Characterization of the oxidation-sulfidation of a preoxidized ODS FeCrAl alloy

Abstract

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