Characterization of nanomaterials dynamics with transmission electron microscope

Jacob Smith, Sihan Wang, Tim B. Eldred, Cierra DellaRova, Wenpei Gao

Research output: Chapter in Book/Report/Conference proceedingChapterpeer-review

2 Scopus citations

Abstract

Properties and functions of nanomaterials, especially catalysts, are determined by their structure and its interplay with chemical, electrical, mechanical stimuli, and other media. Significant improvement in understanding nanomaterials structures and dynamics at the atomic scale has been made due to the advancement of new instrumentation and methods in electron microscopy. In this article we review the critical progresses made in visualizing the reaction at the solid-liquid interface using liquid cell in TEM, in probing the solid-state chemistry using dose-efficient and high speed electron detectors, and in characterizing the nanoparticle response to gas environment using gas cell and environmental electron microscopy, and discuss how imaging the dynamics with high resolution helps with the design and fabrication of new nanomaterials.

Original languageEnglish
Title of host publicationEncyclopedia of Nanomaterials
PublisherElsevier
PagesV2-123-V2-145
ISBN (Electronic)9780128224236
DOIs
StatePublished - Jan 1 2023
Externally publishedYes

Bibliographical note

Publisher Copyright:
© 2023 Elsevier Inc. All rights reserved.

Keywords

  • Atomic resolution
  • Catalyst
  • Dynamics
  • Environmental TEM
  • Gas cell
  • In situ electron microscopy
  • Liquid cell
  • Nanoparticle growth
  • Scanning transmission electron microscopy
  • STEM

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