Characterization of Al-Mg Alloy Aged at Low Temperatures

Gaosong Yi, David A. Cullen, Kenneth C. Littrell, William Golumbfskie, Erik Sundberg, Michael L. Free

Research output: Contribution to journalArticlepeer-review

41 Scopus citations

Abstract

Long-term aged [343 K (70 °C) for 30 months and natural exposure for over 10 years] Al 5456 H116 samples were characterized using electron backscatter diffraction (EBSD), scanning transmission electron microscopy (STEM), state-of-the-art energy-dispersive X-ray spectroscopy (EDS) systems, and small-angle neutron scattering (SANS). ASTM G-67 mass loss tests of the sensitized Al 5456 alloy samples were conducted. Intragranular Mg-rich precipitates, such as Guinier–Preston (GP) zones, were confirmed in Al 5456 H116 aged at 343 K (70 °C) for 30 months, and the volume of these precipitates is 1.39 pct. β′ phase is identified at the grain boundary of a navy ship sample, while high-resolution STEM results reveal no intragranular precipitates. Intergranular corrosion (IGC) of Al 5456 was found to be related to the continuity of intergranular precipitates.

Original languageEnglish
Pages (from-to)2040-2050
Number of pages11
JournalMetallurgical and Materials Transactions A: Physical Metallurgy and Materials Science
Volume48
Issue number4
DOIs
StatePublished - Apr 1 2017

Funding

The work is supported by Office of Naval Research, Award Number: N000141210507. A portion of this research was conducted at the Center for Nanophase Materials Sciences, which is a DOE Office of Science User Facility. This work utilizes the Oak Ridge National Laboratory’s High Flux Isotope Reactor, which is sponsored by the Scientific User Facilities Division, Office of Basic Energy Sciences, U.S. Department of Energy. This work made use of University of Utah USTAR shared facilities support, in part, by the MRSEC Program of NSF under Award No. DMR-1121252.

FundersFunder number
Oak Ridge National Laboratory
Scientific User Facilities Division
National Science FoundationDMR-1121252
Office of Naval ResearchN000141210507
U.S. Department of Energy
Basic Energy Sciences

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