Abstract
This study presents the design and implementation of a side entry laser system designed for an ultrahigh vacuum scanning transmission electron microscope. This system uses a versatile probe design enclosed in a vacuum envelope such that parts can be easily aligned, modified or exchanged without disturbing the vacuum. The system uses a mirror mounted on the sample holder such that the sample can be illuminated without being tilted. Notably the mirror can be removed and replaced with an ablation target and a higher power laser used to ablate material directly onto the sample. The authors argue that new capabilities hold the potential to transform the electron microscope from an analysis tool toward a more flexible synthesis system, where atomic scale fabrication and atom-by-atom experiments can be performed.
| Original language | English |
|---|---|
| Article number | 2401208 |
| Journal | Advanced Materials Technologies |
| Volume | 10 |
| Issue number | 5 |
| DOIs | |
| State | Published - Mar 4 2025 |
Funding
Electron microscopy and phase transformation was supported by the U.S. Department of Energy, Office of Science, Basic Energy Sciences, Materials Sciences and Engineering Division (O.D., K.X., A.R.L., S.J.) and was performed at the Oak Ridge National Laboratory's Center for Nanophase Materials Sciences (CNMS), a U.S. Department of Energy, Office of Science User Facility. The Vesta side entry laser accessory described here was developed and produced by Waviks, Inc. (Dallas, TX). B.W. and T.M. have equity interests in Waviks, Inc.
Keywords
- atomic manipulation
- in situ processing
- laser
- laser evaporation
- scanning transmission electron microscope
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