A real-time neutron diffraction study of phase transitions in the Ti-D system after high-pressure treatment

A. I. Kolesnikov, A. M. Balagurov, I. O. Bashkin, V. K. Fedotov, V. Yu Malyshev, G. M. Mironova, E. G. Ponyatovsky

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22 Scopus citations

Abstract

Phase transitions in TiDapproximately 0.75 subjected to high-pressure treatment were investigated by simultaneous real-time measurements of neutron diffraction and small-angle neutron scattering. The neutron spectra were taken on heating the samples in the temperature ranges 100 to 300 K and 300 to 760 K followed by cooling to 430 K. A sequence of structural transitions was observed, which involves seven different phases and intermediate states with the hexagonal close-packed, face-centred cubic, face-centered orthorhombic or body-centred cubic metal sublattices and hydrogen atoms distributed on octahedral or ordered/disordered tetrahedral interstices.

Original languageEnglish
Article number003
Pages (from-to)5045-5058
Number of pages14
JournalJournal of Physics Condensed Matter
Volume5
Issue number29
DOIs
StatePublished - 1993
Externally publishedYes

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