Abstract
A new diffractometer is now available to the general user community at the ESRF. The new diffractometer is a side station of the high-resolution inelastic X-ray scattering spectrometer on beamline ID28 and is located in the same experimental hutch. Both instruments can be operated simultaneously. The new diffractometer combines a fast and low-noise hybrid pixel detector with a variable diffraction geometry. The beam spot on the sample is 50 µm × 50 µm, where focusing is achieved by a combination of Be lenses and a KB mirror. Wavelengths from 0.5 to 0.8 Å can be used for the diffraction experiments. The setup is compatible with a variety of sample environments, allowing studies under non-ambient conditions. The diffractometer is optimized to allow a rapid survey of reciprocal space and diffuse scattering for the identification of regions of interest for subsequent inelastic scattering studies, but can also be employed as a fully independent station for structural studies from both powder and single-crystal diffraction experiments. Several software packages for the transformation and visualization of diffraction data are available. An analysis of data collected with the new diffractometer shows that the ID28 side station is a state-of-the-art instrument for structural investigations using diffraction and diffuse scattering experiments.
Original language | English |
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Pages (from-to) | 272-279 |
Number of pages | 8 |
Journal | Journal of Synchrotron Radiation |
Volume | 26 |
Issue number | 1 |
DOIs | |
State | Published - Jan 2019 |
Externally published | Yes |
Funding
This study was supported by the BMBF project 05K13RF1 and 05K13RF2 and a joint DFG-ANR project WI1232/41-1.
Funders | Funder number |
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DFG-ANR | WI1232/41-1 |
Bundesministerium für Bildung und Forschung | 05K13RF1, 05K13RF2 |
Keywords
- X-ray diffuse scattering
- diffraction
- disorder
- inelastic X-ray scattering
- phonons