A facile high-speed vibration milling method to water-disperse singlewalled carbon nanohorns

Chunying Shu; Jianfei Zhang; Jiechao Ge; Jae Hyun Sim; Brian G. Burke; Keith A. Williams; Nichole M. Rylander; Tom Campbell; Alex Puretzky; Chris Rouleau; David B. Geohegan; Karren More; Alan R. Esker; Harry W. Gibson; Harry C. Dorn

doi:10.1021/cm902710n

A facile high-speed vibration milling method to water-disperse singlewalled carbon nanohorns

Chunying Shu, Jianfei Zhang, Jiechao Ge, Jae Hyun Sim, Brian G. Burke, Keith A. Williams, Nichole M. Rylander, Tom Campbell, Alex Puretzky, Chris Rouleau, David B. Geohegan, Karren More, Alan R. Esker, Harry W. Gibson, Harry C. Dorn

Research output: Contribution to journal › Article › peer-review

24 Scopus citations

Abstract

A high-speed vibration milling (HSVM) method was applied to synthesize water dispersible singlewalled carbon nanohorns (SWNHs). Highly reactive free radicals (HOOCCH ₂CH ₂•) produced from an acyl peroxide under HSVM conditions react with hydrophobic SWNHs to produce a highly water dispersible derivative (f-SWNHs), which has been characterized in detail by spectroscopic and microscopic techniques together with thermogravimetric analysis (TGA) and dynamic light scattering (DLS). The carboxylic acid functionalized, water-dispersible SWNHs material are versatile precursors that have potential applications in the biomedical area.

Original language	English
Pages (from-to)	347-351
Number of pages	5
Journal	Chemistry of Materials
Volume	22
Issue number	2
DOIs	https://doi.org/10.1021/cm902710n
State	Published - Jan 26 2010

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Shu, C., Zhang, J., Ge, J., Sim, J. H., Burke, B. G., Williams, K. A., Rylander, N. M., Campbell, T., Puretzky, A., Rouleau, C., Geohegan, D. B., More, K., Esker, A. R., Gibson, H. W., & Dorn, H. C. (2010). A facile high-speed vibration milling method to water-disperse singlewalled carbon nanohorns. Chemistry of Materials, 22(2), 347-351. https://doi.org/10.1021/cm902710n

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abstract = "A high-speed vibration milling (HSVM) method was applied to synthesize water dispersible singlewalled carbon nanohorns (SWNHs). Highly reactive free radicals (HOOCCH 2CH 2•) produced from an acyl peroxide under HSVM conditions react with hydrophobic SWNHs to produce a highly water dispersible derivative (f-SWNHs), which has been characterized in detail by spectroscopic and microscopic techniques together with thermogravimetric analysis (TGA) and dynamic light scattering (DLS). The carboxylic acid functionalized, water-dispersible SWNHs material are versatile precursors that have potential applications in the biomedical area.",

author = "Chunying Shu and Jianfei Zhang and Jiechao Ge and Sim, {Jae Hyun} and Burke, {Brian G.} and Williams, {Keith A.} and Rylander, {Nichole M.} and Tom Campbell and Alex Puretzky and Chris Rouleau and Geohegan, {David B.} and Karren More and Esker, {Alan R.} and Gibson, {Harry W.} and Dorn, {Harry C.}",

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T1 - A facile high-speed vibration milling method to water-disperse singlewalled carbon nanohorns

AU - Shu, Chunying

AU - Zhang, Jianfei

AU - Ge, Jiechao

AU - Sim, Jae Hyun

AU - Burke, Brian G.

AU - Williams, Keith A.

AU - Rylander, Nichole M.

AU - Campbell, Tom

AU - Puretzky, Alex

AU - Rouleau, Chris

AU - Geohegan, David B.

AU - More, Karren

AU - Esker, Alan R.

AU - Gibson, Harry W.

AU - Dorn, Harry C.

PY - 2010/1/26

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AB - A high-speed vibration milling (HSVM) method was applied to synthesize water dispersible singlewalled carbon nanohorns (SWNHs). Highly reactive free radicals (HOOCCH 2CH 2•) produced from an acyl peroxide under HSVM conditions react with hydrophobic SWNHs to produce a highly water dispersible derivative (f-SWNHs), which has been characterized in detail by spectroscopic and microscopic techniques together with thermogravimetric analysis (TGA) and dynamic light scattering (DLS). The carboxylic acid functionalized, water-dispersible SWNHs material are versatile precursors that have potential applications in the biomedical area.

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A facile high-speed vibration milling method to water-disperse singlewalled carbon nanohorns

Abstract

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